Resultados de investigación

6 pages. -- Figure S1. Pb 4f and S 2p high resolution XPS spectra obtained from the PbS nanoparticles. -- Figure S2. XRD patterns of PbS nanoparticles with and without H2-reducing treatment. -- Figure S3. SEM images and EDX spectra of a) PbS nanoparticles and b) PbS powders after annealing at 600℃ for 3h with H2/Ar atmosphere. -- Figure S4. Histograms of the grain size distribution obtained from the cross section SEM image of the a) PbS pellet without reduction process, and b) PbS pellet with reduction process. SEM images are shown in Figure 3. -- Figure S5. XRD patterns of the Pb1-xCuxS a) nanoparticles and b) annealed powder. -- Figure S6. a) XRD patterns of the SPS sintered Pb1-xCuxS pellets; b) Expanded view of the regions corresponding to the PbS (200) diffraction peak. -- Figure S7. The function of the Cu concentration on the lattice parameters of the Pb1-xCuxS pellets: a) Lattice parameter a=b=c (Å); b) Volume of Cell (Å 3). -- Figure S8. Cross-section SEM image and EDX compositional maps of a Pb0.955Cu0.045S pellet. -- Figure S9. EELS chemical composition maps obtained from the red squared area of the STEM micrograph of the Pb0.955Cu0.045S pellet. -- Table S1. Pb1-xCuxS nanoparticle composition as measured by SEM-EDX and crystal domain size as obtained from XRD data using Scherrer equation. -- Table S2. Hall charge carrier concentration (n), mobility () and effective mass (m*) of Pb1- xCuxS pellets at room temperature., Peer reviewed

Datos geoespaciales en rejilla sobre sequía repentina., [ES] El dataset FlashDroughtMonitor se actualiza periódicamente, se puede consultar y descargar en el siguiente enlace: https://flash-drought.csic.es/ [EN] The FlashDroughtMonitor dataset is updated periodically, it can be consulted and downloaded at the following link: https://flash-drought.csic.es/, [EN] This dataset provides near real-time information about flash drought conditions in Spain with a 1.1 km spatial resolution and weekly frequency. Flash drought onset and spatial extend is identified based on SPEI at short time-scale (1-month)., [ES] Este dataset proporciona información en tiempo cuasi real sobre las condiciones de sequía repentina en España con una resolución espacial de 1.1 km y una frecuencia temporal semanal. El inicio y extensión espacial de la sequía repentina es identificado en base al SPEI a una escala temporal corta (1-mes)., Spanish Commission of Science and Technology and FEDER by the projects PCI2019-103631 and PID2019-108589RA-I00, Consejo Superior de Investigaciones Científicas (España) by the LINKB20080 of the program i-LINK 2021, AXIS (Assessment of Cross(X) - sectoral climate Impacts and pathways for Sustainable transformation), JPI-Climate co-funded call of the European Commission by the CROSSDRO, Peer reviewed

DRX100/extract_xy_euler3-10.txt, extract_xy_euler3-20.txt extract_xy_euler3-30.txt extract_xy_euler3-33.txt extract_xy_euler3-40.txt extract_xy_euler3-50.txt extract_xy_euler3-60.txt extract_xy_euler3-67.txt extract_xy_euler3-70.txt extract_xy_euler3-80.txt extract_xy_euler3-90.txt extract_xy_euler3-100.txt extract_xy_euler3-110.txt extract_xy_euler3-120.txt extract_xy_euler3-1330.txt ELLE200/extract_xy_euler3-10.txt, extract_xy_euler3-20.txt extract_xy_euler3-30.txt extract_xy_euler3-33.txt extract_xy_euler3-40.txt extract_xy_euler3-50.txt extract_xy_euler3-60.txt extract_xy_euler3-67.txt extract_xy_euler3-70.txt extract_xy_euler3-80.txt extract_xy_euler3-90.txt extract_xy_euler3-100.txt extract_xy_euler3-110.txt extract_xy_euler3-120.txt extract_xy_euler3-1330.txt ELLE300/extract_xy_euler3-10.txt, extract_xy_euler3-20.txt extract_xy_euler3-30.txt extract_xy_euler3-33.txt extract_xy_euler3-40.txt extract_xy_euler3-50.txt extract_xy_euler3-60.txt extract_xy_euler3-67.txt extract_xy_euler3-70.txt extract_xy_euler3-80.txt extract_xy_euler3-90.txt extract_xy_euler3-100.txt extract_xy_euler3-110.txt extract_xy_euler3-120.txt extract_xy_euler3-1330.txt ODF_EBSD_GB_halite.m, The way in which salt flows is highly heterogeneous and results in complex fabrics and structures. To improve our understanding of how halite deforms and recrystallizes under different conditions we performed full-field numerical modelling of polycrystalline aggregates of halite. The numerical approach is based on the coupling of the viscoplastic Full-Field Transform code (VPFFT, Lebensohn and Rollet, 2020) that simulates the viscoplastic deformation and multi-scale platform ELLE (Bons et al, 2008) that has enabled recrystallization processes such as recovery, nucleation and grain boundary migration. This data set This data set contains (i) the output files with the crystal orientation data of simulation DRX_100, DRX_200 and DRX_300, and (ii) a code to plot the crystallographic orientation density function (ODF) using the open-source code MTEX (Mainprice et al., 2011)., EGR acknowledges the support of the Ramón y Cajal fellowship (RYC2018-026335-I), funded by the MCIN/AEI/10.13039/501100011033 and the FSE. MGL acknowledges the support of the Q2818002D project, funded by MCIN/AEI/10.13039/501100011033 by European Union NextGenerationEU/PRTR., Peer reviewed

6 pages. -- Figure S1. Picture of the MEA ERG probes after being used to measure ERG. -- Figure S2. Electrochemical Impedance Spectroscopy Bode plot of 5 of the graphene microelectrodes after measurements such as those described in Figure 3 a). S. -- Figure S3. ERG measured with the linear MEA showing different signal amplitudes across the probe. -- Figure S4. Optical transmittance measurement of the head of a circular MEA probe over the visible range. -- Figure S5. MEA ERG recordings from a healthy animal (top) and an animal with a lesion in the temporal-ventrical quadrant of the retina., Peer reviewed

5 pages. -- ESI-Figure 1: XRD pattern of L2NO4 thin films with different thickness deposited at 650 °C on a) LAO, b) STO and c) YSZ. Substrate peaks are marked by grey dots and the observed L2NO4 planes are labelled according to ICDD reference 04-015-2147. -- ESI-Figure 2: c-parameter as a function of thickness for ”as-deposited“ L2NO4 films on LAO and STO single crystal substrates. -- ESI-Figure 3: Grain size distribution, i.e. number of grains for each grain size, for all L2NO4 film thicknesses and substrates, analysed within an area of 1.13×0.76 µm. -- ESI-Figure 4: SEM analysis of 200 nm thick L2NO4 film deposited at 750 °C on a) LAO and b) YSZ substrate. -- ESI-Figure 5: Atomic force microscopy of L2NO4/LAO samples, revealing increasing roughness (RMS) from 2.6 to 11.9 nm with increasing film thickness from 33 to 540 nm. -- ESI-Figure 6: STEM EDX analysis of 540 nm thick L2NO4/LAO sample. -- ESI-Figure 7: Analysis of microstructural stability of L2NO4 by SEM and XRD after functional characterisation at temperatures up to 600 °C with a total annealing duration of 24h. -- ESI-Figure 8: Normalised conductivity transients of L2NO4 thin films at 375°C after a change of pO2 from 10-250 mbar. -- ESI-Figure 9: a) Electrochemical impedance spectroscopy of nano-columnar L2NO4/YSZ measured in dry air in the frequency range from 1 MHz to 1 Hz at 590 °C. The equivalent circuit, used to fit the EI spectra, is shown in the inset, with a resistive contribution for YSZ in series to a high and low frequency Randles cell for the counter and the L2NO4 working electrode, respectively. b) L2NO4 contribution over the reciprocal temperature for 100 and 200 nm thick L2NO4., Peer reviewed

2 pages. -- Fig. S1. Summary of the procedure: (i) First, equivalent circuit of the halide perovskite is found from impedance measurements, monitoring, in addition, the parameters that describe the response at different applied bias voltages. Typically, a CPE behavior is found in the low-frequency region. (ii) From the correlation of impedance spectroscopy and transient analysis, the trend of the potential-step hold time is determined using fractional calculus, in order to find the most restrictive condition and thus achieve steady-state conditions (refer to Eq. (12)). (iii) Finally, the critical scan rate is calculated from Eq. (13)., Peer reviewed

11 pages. -- Figure S1. Schematic of the inkjet-printed conductivity and volume sensors and of the SPCE device with the respective measurements. -- Calculation of the k value from the conductivity and volume nanobiosensors. -- Table S1. Comparison with other heavy metal and conductivity sensors for sweat analysis. -- Battery consumption. -- Voltage increment limitations of the LMP91000 chip. -- Copper detection pH dependence. -- Repeatability of the copper detection for continuous monitoring. -- Figure S2. SPCE device tested continuously in 1400 ppb copper in artificial sweat for 25 measurements during 95 min (without any cleaning between each single measurement). -- Sensors parameters optimization. -- Figure S3. Bode diagrams of the conductivity (a) and volume (b) sensors with the microchannel filled by NaCl 95 mM in milliQ water, emulating the sweat conductivity. -- Figure S4. Schematic illustration of different sampling time with respect to the imposed potential and the measured currents (a) and stripping curves using different sampling time (b). -- Bending effects. -- Figure S5. The microfluidic device applied on the distal arm skin., Peer reviewed

23 pages. -- PDF file includes: I. Literature Review on Electrical and Structural Properties of Ferroelectric Thin Film. -- II. Coercive Field in BaTiO3 Thin Films Grown on SrTiO3/Si Substrates. -- I. Structural Characterization of BaTiO3 Thin Films Grown at Different Pressures. -- II. Polarization-Electric Field Hysteresis Loops of BaTiO3 Films. -- III. Stoichiometry Characterization. -- IV. Study of Different Electrode Synthesis and Fabrication Processes. -- V. Scanning Transmission Electron Microscopy Studies. -- VI. Structural Characterization of 125-225 nm BaTiO3 Thin Films. -- VII. Reciprocal Space Mapping of 12.5-100 nm BaTiO3 Thin Films Grown at 60 mTorr. -- VIII. Polarization-Voltage/Electric Field Hysteresis Loops of BaTiO3 Thin Films. -- IX. Piezoresponse Force Microscopy Scans of 25-nm-thick BaTiO3 Thin Film. -- X. Fatigue and Retention Measurements. -- XI. Switching-Dynamics Measurements on 25 nm BaTiO3 Thin Films. -- XII. Lateral Size-Scaling on 50 nm and 100 nm BaTiO3 Thin Films. -- XIII. Structural Characterization of BaTiO3 Grown on SrTiO3/Si Substrates. -- XIV. Dielectric Constant-Voltage Measurement, Peer reviewed

14 pages. -- PDF file includes: Details of Theoretical calculations. -- Figure S1. (a) SEM images of the Bi2Se3 nanosheets. (b) XRD patterns of Bi2Se3 nanosheets. (c) HRTEM images of the Bi2Se3 nanosheets and its corresponding power spectrum. (d) EELS chemical composition maps obtained from the red squared area of the STEM micrograph. -- Figure S2. Bi 4f and Se 3d high-resolution XPS spectra. -- Figure S3. XRD pattern of I-Bi2Se3/S. -- Figure S4. TGA curve of I-Bi2Se3/S composite measured in N2 with a sulfur loading ratio of 70.2 wt%. -- Figure S5. Nitrogen adsorption-desorption isotherms of as synthesized I-Bi2Se3 and IBi2Se3/S composites. -- Figure S6. DFT calculation results of optimized geometrical configurations of the surface (110) of Bi2Se3 with LiPS (Li2S, Li2S2, Li2S4, Li2S6, Li2S8 and S8). -- Figure S7. DFT calculation results of optimized geometrical configurations of the surface (110) of I-Bi2Se3 with LiPS (Li2S, Li2S2, Li2S4, Li2S6, Li2S8 and S8). -- Figure S8. Optimized adsorption configuration of Li2S decomposition on Bi2Se3. -- Figure S9. First five cycles of CV curves of (a) I-Bi2Se3/S, (b) Bi2Se3/S and (c) Super P/S performed at a scan rate of 0.1 mV s−1. -- Figure S10. Differential CV curves of (a) I-Bi2Se3/S, (c) Bi2Se3/S and (e) Super P/S. The baseline voltage and current density are defined as the value before the redox peak, where the variation on current density is the smallest, named as dI/dV=0. -- Figure S11. CV curves of (a) Bi2Se3/S, (b) Super P/S and (c) Plot of CV peak current for peaks C1, C2, and A versus the square root of the scan rates. -- Figure S12. The CV curve of I-Bi2Se3 as electrode measured in symmetric coin cell using an electrolyte without Li2S6. -- Figure S13. (a) Charge, and (b) discharge profiles of I-Bi2Se3/S, Bi2Se3/S, and Super P/S electrodes showing the overpotentials for conversion between soluble LiPS and insoluble Li2S2/Li2S. -- Figure S14. Galvanostatic charge−discharge profiles of (a) Bi2Se3/S and (b) Super P/S at different current densities range from 0.1C to 4C. -- Figure S15. (a,b) EIS spectra of (a) Bi2Se3/S and (b) Super P/S coin cells before and after cycling. The solid line corresponding to the fitting result from the equivalent circuit (c) and (d), and the Rs, Rin, Rct, and Zw stand for the resistance of the electrolyte, insoluble Li2S2/Li2S layer, interfacial charge-transportation, and semi-infinite Warburg diffusion, respectively; and CPE stands for the corresponding capacitance. (e) Different resistances of three coin cells were obtained from the equivalent circuit. -- Figure S16. XRD patterns of electrode materials after 100 cycles at 1C. -- Figure S17. Galvanostatic charge/discharge profiles of I-Bi2Se3/S at 0.5C under a lean electrolyte condition with a high sulfur loading of 5.2 mg cm-2. -- Figure S18. (a) SEM image of the Li-anode after cycling; (b) EDX mapping image of Lianode showing sulfur signal after cycling. -- Figure S19. SEM image of the cathode material after cycling, EDX spectra and EDX elemental maps for S, Se, Bi and I. -- Figure S20. I-Bi2Se3 optimized configuration as calculated by DFT. The distance between I and Bi is 3.15 Å, which is similar values than the bond lengths in bulk BiI3. -- Table S1 Summary of the comparison of I-Bi2Se3 electrochemical performance as host cathode for LSBs with state-of-the-art Bi-based or Se-based materials., Peer reviewed

18 pages. -- PDF file includes: materials and methods: Production of biotinylated detection antibodies (bd-MAb). -- Figure S-1. MP functionalization with c-MAb. -- Figure S-2. S-2. Scheme and protocol of the reference sandwich ELISA for Pf-LDH detection. -- Figure S-3. Two-step magneto-immunoassay for Pf-LDH detection. -- Figure S-4. Single-step magneto-immunoassay for Pf-LDH detection: comparison of colorimetric and fluorescent detection. -- Figure S-5. Performance of the 9 membranes studied. -- Figure S-6. Optimization of MP washing on-chip. -- Figure S-7. Optimization of the paper-based detection strategy. -- Figure S-8. Detection of malaria in positive blood samples using a commercial RDT. -- Table S-1. Examples of magneto immunoassays reported before for malaria diagnosis. -- Table S-2. Characteristics of the 9 paper-like membranes tested. -- Table S-3. Summary of results obtained in malaria-positive clinical samples using the paperbased fluorescence POC and reference ELISA, microscopy and RDT methodologies. -- Table S-4. Estimated production cost for each paper-based magneto-immunoassay test., Peer reviewed