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Source data for the article entitle "Interchain Expanded Extra-Large Pore Zeolites", Nature 2024, including the detailed structural and physicochemical and chemical characterization of those zeolites, [EN] 1. Description of methods used for collection/generation of data: Diffraction (electron, synchrotron X-ray, neutron). Infrared spectroscopy multinuclear MAS NMR gas adsorption electron paramagnetic resonance DFT calculations Catalytic reaction 2. Methods for processing the data: Those needed depending on the type of data (SHELX, Rietveld refinement, fast Fourier Transform...). Please, check the paper., Spanish Ministry of Science Innovation, PID2019-105479RB-I00, TED2021-131223B-I00 projects, and RYC2018-024561-I and FJC2018-035697-I National Natural Science Foundation of China, 22371121, 22288101, 21920102005, 21835002, 22271115 and 52270111 National Key Research and Development Program of China, 2022YFA1503600, 2021YFA1501202, 2021YFA1501401 the 111 project, B17020 Fundamental Research Funds for the Central Universities of China, 020514380306 Consejería de Universidades, Investigación e Innovación, Junta de Andalucía, POSTDOC_21_00069 Knut and Alice Wallenberg Foundation, KAW, 2012-0112 European Union’s Horizon 2020 research and innovation program, 823717-ESTEEM3 regional government of Aragon, DGA E13_20R China Spallation Neutron Source, P1823060200002, Fig-2.xlsx; Ex-Fig1.xlsx; Ex-Fig. 3.xlsx; Ex-Fig. 6.xlsx; Ex-Fig. 7.xlsx; Ex-Fig. 8.xlsx; Fig-S8.xlsx; Fig-S9.xlss; Fig-S10.xlsx Fig-S11.xlsx Fig-S12.xlsx Fig-S13.xlsx Fig-S14.xlsx Fig-S15.xlsx Fig-S16a.csv Fig-S16b.csv Fig-S17.csv Fig-S18.xlsx; Fig-S19.csv; Fig-S20.xlsx; Fig-S21.xlsx; Fig-S22a.csv; Fig-S22b.csv; Fig-S23.xlsx; Fig-S24.xlsx; Fig-S25.xlsx, No