BUSCADOR RECOLECTA

Data base containing SPME-GC-MS raw analytical data obtained and used by Quintanilla-Casas et al. (Food Chemistry, 2020, 125556). Data correspond to 82 authentic and traceable olive oil samples, declared as EVOO by the suppliers obtained in the framework of OLEUM project (EC H2020 Programme 2014–2020) from seven different EU and non-EU countries: Croatia (n=11); Slovenia (SVN) (n=8); Spain (ESP) (n=17); Italy (ITA) (n=15); Greece (GRC) (n=6); Morocco (MAR) (n=15) and Turkey (TUR) (n=10). With the aim of reflecting the real production scenario, EVOO samples in this prospective study were obtained under usual production practices for commercial purposes, and thus consisted of both monovarietal oils as well as market blends of olive cultivars typical of each geographical origin. Briefly, data correspond to SPME-GC-MS scan intensities of the specific sesquiterpene hydrocarbon (SH) ions (m/z 93, 107, 119, 135, 157, 159, 161, 189 and 204) obtained from the Total Ion Current (TIC) between the 18th to the 30th minute. Thus, 2467 scans were obtained for each m/z ion implying 22203 variables per sample.

Data base containing data on the triacylclgyerol profile of genuine and adulterated olive oils obtained by Flow Injection Analysis-Heated Electrospray Ionisation-High Resolution Mass Spectrometry (FIA-HESI-HRMS). Data (total ion chromatograms) were obtained and used by Quintanilla-Casas et al. (Food Control, 2021, 123: 107851). Data correspond to relative abundances obtained for each mass signal that agreed with single positive charged sodium molecular ions and that could match with a triacylglycerol elemental formula (mass tolerance error set at 5ppm; molecular formulae calculation performed with Xcalibur 4.1. (Thermo Fisher Scientific, Bremen, Germany). This data base includes samples used in the study that were obtained by the OLEUM consortium. Samples included genuine olive oils, as well as Taylor-made adulterations blending genuine olive oils with other vegetable oils as adulterants (sunflower oli; soy oil; high oleic sunflower oil; avocado oil (refined and virgin); hazelnut oil (refined and virgin)). Blind samples are also included in the data base. Partial Least Squares-Discriminant Analysis (PLS-DA) was applied to these data to develop two independent binary models that discriminated between (i) genuine oils and blends with ≥2% of HL adulterants, and (ii) genuine oils and blends with ≥5% of HO adulterants, as described in Quintanilla-Casas et al., 2021.

Dataset containing SPME-GC-MS raw analytical data (total ion chromatograms, not aligned) obtained and used by Quintanilla-Casas et al. (LWT - Food Science and Technology 121: 108936). Data correspond to the volatile fingerprint of 174 authentic and traceable virgin olive oil samples previously graded by six official sensory panels (data from 2 outlier samples are not included) in the framework of OLEUM project (EC H2020 Programme 2014–2020). Briefly, data correspond to SPME-GC-MS scan intensities of the total ion chromatogram at each retention time from 5.5 to 61.96 min. These data were aligned and used under a fingerprinting approach by Quintanilla-Casas et al. to develop a classification model (PLS-DA approach) to verify the sensory quality of virgin olive oils, and it was suggested as an instrumental method to support sensory panels.

TOROS-III Cruise (29GD19970610) carried out on the Research Vessel García del Cid in 1997, Tinto and Odiel River-Ocean Study.The surveys were designed to study the trace metal and nutrient biogeochemistry in the coastal waters influenced by the discharges of the rivers Guadiana, Tinto, Odiel and Guadalquivir which drain parts of the southern Iberian Peninsula.High spatial resolution data for dissolved Cu, Ni, Zn and Co were obtained in the Gulf of Cadiz on-board the research vessel Garcia del Cid.Continuous underway sampling at ca. 2 m depth was carried out using a fish towed from a crane on the Garcia del Cid

TOROS-IV Cruise (29GD19981011) carried out on the Research Vessel García del Cid in 1998, Tinto and Odiel River-Ocean Study.The surveys were designed to study the trace metal and nutrient biogeochemistry in the coastal waters influenced by the discharges of the rivers Guadiana, Tinto, Odiel and Guadalquivir which drain parts of the southern Iberian Peninsula.High spatial resolution data for dissolved Cu, Ni, Zn and Co were obtained in the Gulf of Cadiz on-board the research vessel Garcia del Cid.Continuous underway sampling at ca. 2 m depth was carried out using a fish towed from a crane on the Garcia del Cid

YOYO-I Cruise (29GD19990505) carried out on the Research Vessel García del Cid in 1999, The YOYO project aims to develop a system of automatic measurement of the marine environment by building a series of sensors and analyzer modules

YOYO-II Cruise (29G19991014) carried out on the Research Vessel García del Cid in 1999, Bathymetry in the area near the fixed point, realization of a profile with the Rossete / CTD and sampling of the Niskin bottles in the fixed point, Installation and start of the monitoring of the silicate sensor in the YOYO system. In situ control of the sensor

OAMMS-1 Cruise (29GD20090309) carried out on the Research Vessel García del Cid in 2009, Observation, Analysis and Modelling of the Mediterranean Sea(OMMS).The main objective is to consolidate a system of observation of the Mediterranean Sea through the real-time measurement of a number of meteorological and oceanographic magnitudes with a moored buoy, complemented by periodic visits with a research vessel to the mooring site and assimilation of the observations obtained in order to carry out the systematic forecasting of sea conditions in the NW Mediterranean Sea.Six-monthly visits from the R/V Garcia del Cid will be performed at the mooring site and at a grid covering parts of the Catalan Sea. On-deck inspection and maintenance of the instrumentation on the buoy will be carried out. The system was equipped with: a. Positional (GPS, ARGOS transmitter) and meteorological sensors (radiation, wind direction and speed -2 units-, air temperature -2 units-, relative humidity and air pressure). b. Sea surface sensor (temperature, salinity) and ADCP downward looking current meter. c. Underwater sensors -2 units- (depth, temperature, salinity, dissolved oxygen, fluorescence, turbidity, photosynthetic active radiation –PAR-). d. Data logging (Campbell Scientific) and system control. e. transmitting (two-way GSM modem connection) to the shore The proposed research project also aims at consolidating an observational system based on the CEAB multiparametric buoy, equipped with meteorological and oceanographic sensors for real time measurement and transmission to shore of the atmospheric and marine conditions. The buoy will be moored from the B/O García del Cid at a fixed point in the catalan coast, at the head of the Blanes canyon. Automatic observations will be complemented by a series of visits with the CEAB boat to the station where the buoy is moored in order to gather water and plankton samples. At the same time, the present procedure will be improved for the acquisition of water color data (chlorophyll, yellow substance, suspended particles) obtained by the MERIS sensor on board ESA’s ENVISAT satellite. These data offer two levels: 1) real time high spacial resolution files for the western Mediterranean Sea (Levels 1 and 2); and 2) global low to medium spacial resolution (Level 3). The data, together with other historical data also available, will constitute the project database with public access installed in the CEAB server. Limited access will be granted to users in general and, under request, to those with justified scientific or educational interests. A protocol for quality control of the data will be established and followed by statistical analysis in order to provide the models with a sound observational base for their calibration and validation

OAMMS-2 Cruise (29GD20090915) carried out on the Research Vessel García del Cid in 2009, Observation, Analysis and Modelling of the Mediterranean Sea(OMMS).The main objective is to consolidate a system of observation of the Mediterranean Sea through the real-time measurement of a number of meteorological and oceanographic magnitudes with a moored buoy, complemented by periodic visits with a research vessel to the mooring site and assimilation of the observations obtained in order to carry out the systematic forecasting of sea conditions in the NW Mediterranean Sea.Six-monthly visits from the R/V Garcia del Cid will be performed at the mooring site and at a grid covering parts of the Catalan Sea. On-deck inspection and maintenance of the instrumentation on the buoy will be carried out. The system was equipped with: a. Positional (GPS, ARGOS transmitter) and meteorological sensors (radiation, wind direction and speed -2 units-, air temperature -2 units-, relative humidity and air pressure). b. Sea surface sensor (temperature, salinity) and ADCP downward looking current meter. c. Underwater sensors -2 units- (depth, temperature, salinity, dissolved oxygen, fluorescence, turbidity, photosynthetic active radiation –PAR-). d. Data logging (Campbell Scientific) and system control. e. transmitting (two-way GSM modem connection) to the shore The proposed research project also aims at consolidating an observational system based on the CEAB multiparametric buoy, equipped with meteorological and oceanographic sensors for real time measurement and transmission to shore of the atmospheric and marine conditions. The buoy will be moored from the B/O García del Cid at a fixed point in the catalan coast, at the head of the Blanes canyon. Automatic observations will be complemented by a series of visits with the CEAB boat to the station where the buoy is moored in order to gather water and plankton samples. At the same time, the present procedure will be improved for the acquisition of water color data (chlorophyll, yellow substance, suspended particles) obtained by the MERIS sensor on board ESA’s ENVISAT satellite. These data offer two levels: 1) real time high spacial resolution files for the western Mediterranean Sea (Levels 1 and 2); and 2) global low to medium spacial resolution (Level 3). The data, together with other historical data also available, will constitute the project database with public access installed in the CEAB server. Limited access will be granted to users in general and, under request, to those with justified scientific or educational interests. A protocol for quality control of the data will be established and followed by statistical analysis in order to provide the models with a sound observational base for their calibration and validation

OAMMS-3 Cruise (29GD20100301) carried out on the Research Vessel García del Cid in 2010, Observation, Analysis and Modelling of the Mediterranean Sea(OMMS).The main objective is to consolidate a system of observation of the Mediterranean Sea through the real-time measurement of a number of meteorological and oceanographic magnitudes with a moored buoy, complemented by periodic visits with a research vessel to the mooring site and assimilation of the observations obtained in order to carry out the systematic forecasting of sea conditions in the NW Mediterranean Sea.Six-monthly visits from the R/V Garcia del Cid will be performed at the mooring site and at a grid covering parts of the Catalan Sea. On-deck inspection and maintenance of the instrumentation on the buoy will be carried out. The system was equipped with: a. Positional (GPS, ARGOS transmitter) and meteorological sensors (radiation, wind direction and speed -2 units-, air temperature -2 units-, relative humidity and air pressure). b. Sea surface sensor (temperature, salinity) and ADCP downward looking current meter. c. Underwater sensors -2 units- (depth, temperature, salinity, dissolved oxygen, fluorescence, turbidity, photosynthetic active radiation –PAR-). d. Data logging (Campbell Scientific) and system control. e. transmitting (two-way GSM modem connection) to the shore The proposed research project also aims at consolidating an observational system based on the CEAB multiparametric buoy, equipped with meteorological and oceanographic sensors for real time measurement and transmission to shore of the atmospheric and marine conditions. The buoy will be moored from the B/O García del Cid at a fixed point in the catalan coast, at the head of the Blanes canyon. Automatic observations will be complemented by a series of visits with the CEAB boat to the station where the buoy is moored in order to gather water and plankton samples. At the same time, the present procedure will be improved for the acquisition of water color data (chlorophyll, yellow substance, suspended particles) obtained by the MERIS sensor on board ESA’s ENVISAT satellite. These data offer two levels: 1) real time high spacial resolution files for the western Mediterranean Sea (Levels 1 and 2); and 2) global low to medium spacial resolution (Level 3). The data, together with other historical data also available, will constitute the project database with public access installed in the CEAB server. Limited access will be granted to users in general and, under request, to those with justified scientific or educational interests. A protocol for quality control of the data will be established and followed by statistical analysis in order to provide the models with a sound observational base for their calibration and validation